D-Deoxyrhamnojirimycin hydrochloride

Base Information

Chemical Name:D-Deoxyrhamnojirimycin hydrochloride
CAS No.:142204-08-8
Molecular Formula:C₆H₁₃NO₃*ClH
Molecular Weight:183.635
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-Deoxyrhamnojirimycin hydrochloride

Chemical Property:

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Technology Process of D-Deoxyrhamnojirimycin hydrochloride

There total 6 articles about D-Deoxyrhamnojirimycin hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94840-08-1
2,3-O-isopropylidene-L-gulono-γ-lactone

: 142204-08-8,210174-73-5
D-Deoxyrhamnojirimycin hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 72 percent / CBr₄, triphenylphosphine / tetrahydrofuran / a) 0 deg C to r.t., 2 h, b) r.t., 10 h

2: 86 percent / H₂, Et₃N / 10percent Pd/C / ethanol / 3 h

3: pyridine / CH₂Cl₂ / 1 h / -20 °C

4: NaN₃ / dimethylformamide / 24 h / Ambient temperature

5: 89 percent / H₂ / 10percent Pd/C / methanol / 5 h

6: 1) Me₂S*BH₃, 2) aq.conc.HCl / 1) THF, 12 h, 2) EtOH, 12 h, -20 deg C

With pyridine; hydrogenchloride; sodium azide; carbon tetrabromide; dimethylsulfide borane complex; hydrogen; triethylamine; triphenylphosphine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(92)85012-4

Reference yield:

: 142204-13-5
6-Deoxy-2,3-O-isopropylidene-L-gulono-γ-lactone

: 142204-08-8,210174-73-5
D-Deoxyrhamnojirimycin hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / CH₂Cl₂ / 1 h / -20 °C

2: NaN₃ / dimethylformamide / 24 h / Ambient temperature

3: 89 percent / H₂ / 10percent Pd/C / methanol / 5 h

4: 1) Me₂S*BH₃, 2) aq.conc.HCl / 1) THF, 12 h, 2) EtOH, 12 h, -20 deg C

With pyridine; hydrogenchloride; sodium azide; dimethylsulfide borane complex; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(92)85012-4

Reference yield:

: 142204-12-4
6-Bromo-6-deoxy-2,3-O-isopropylidene-L-gulono-γ-lactone

: 142204-08-8,210174-73-5
D-Deoxyrhamnojirimycin hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / H₂, Et₃N / 10percent Pd/C / ethanol / 3 h

2: pyridine / CH₂Cl₂ / 1 h / -20 °C

3: NaN₃ / dimethylformamide / 24 h / Ambient temperature

4: 89 percent / H₂ / 10percent Pd/C / methanol / 5 h

5: 1) Me₂S*BH₃, 2) aq.conc.HCl / 1) THF, 12 h, 2) EtOH, 12 h, -20 deg C

With pyridine; hydrogenchloride; sodium azide; dimethylsulfide borane complex; hydrogen; triethylamine; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(92)85012-4