{Mn2(CO)6(μ-dppm)2}

Base Information

Chemical Name:{Mn2(CO)6(μ-dppm)2}
CAS No.:57403-90-4
Molecular Formula:C₅₆H₄₄Mn₂O₆P₄
Molecular Weight:1046.73
Hs Code.:

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Chemical Property of {Mn2(CO)6(μ-dppm)2}

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Technology Process of {Mn2(CO)6(μ-dppm)2}

There total 5 articles about {Mn2(CO)6(μ-dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 37523-60-7
μ-bis(diphenylphosphino)methane-P:P'-octacarbonyldimanganese(Mn-Mn)

: 917-92-0
3,3-Dimethylbut-1-yne

: 57403-90-4
{Mn2(CO)6(μ-dppm)2}

: Mn2(μ-C=CH(t-Bu))(CO)6(μ-dppm)

: {Mn2(μ-η(1),η(2)-CO)(CO)4(μ-dppm)2}

Guidance literature:: In acetone; Irradiation (UV/VIS); under N2; irradn. (mercury lamp), -20°C, 10 h; removal of solvent, dissolving in THF, filtering through Celite, crystn. from THF-petroleum ether at -20°C overnight, washing with petroleum ether;
DOI:10.1021/om00037a062

Reference yield: 27.0%

: 37523-60-7
μ-bis(diphenylphosphino)methane-P:P'-octacarbonyldimanganese(Mn-Mn)

: 917-92-0
3,3-Dimethylbut-1-yne

: 57403-90-4
{Mn2(CO)6(μ-dppm)2}

: Mn2(μ-H)(μ-η-CC-t-Bu)(CO)6(μ-dppm)

: Mn2(μ-C=CH(t-Bu))(CO)6(μ-dppm)

: {Mn2(μ-η(1),η(2)-CO)(CO)4(μ-dppm)2}

Guidance literature:: In toluene; Irradiation (UV/VIS); under N2; irradn. (mercury lamp), -20°C, 24 h; removal of solvent, chromy. (Al2O3 activity IV, first with petroleum ether, then with petroleum ether-toluene (10:3), then with toluene, then with CH2Cl2);
DOI:10.1021/om00037a062