Technology Process of C53H75NO15
There total 7 articles about C53H75NO15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); hypophosphorous acid; triethylamine;
In
1,4-dioxane;
for 3h;
Heating;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 77 percent / NaHCO3 / toluene
2: 80 percent
3: 1.) AcOH, 2.) DMSO, trifluoroacetic anhydride
4: 1.) NaH, 2.) aq. HCl
5: 82 percent / 4-dimethylaminopyridine / CH2Cl2
6: 51 percent / 50percent aq. H3PO2, Et3N, AIBN / dioxane / 3 h / Heating; other reagent and solvents
With
hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); hypophosphorous acid; sodium hydride; sodium hydrogencarbonate; acetic acid; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
1,4-dioxane; dichloromethane; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) AcOH, 2.) DMSO, trifluoroacetic anhydride
2: 1.) NaH, 2.) aq. HCl
3: 82 percent / 4-dimethylaminopyridine / CH2Cl2
4: 51 percent / 50percent aq. H3PO2, Et3N, AIBN / dioxane / 3 h / Heating; other reagent and solvents
With
hydrogenchloride; dmap; 2,2'-azobis(isobutyronitrile); hypophosphorous acid; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride;
In
1,4-dioxane; dichloromethane;