(S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene

Base Information

Chemical Name:(S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene
CAS No.:318498-29-2
Molecular Formula:C₂₅H₂₃FeO₂P
Molecular Weight:442.277
Hs Code.:

Synonyms:

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Chemical Property of (S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene

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Technology Process of (S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene

There total 2 articles about (S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: (S,S(p))-1-diphenylphosphanyl-2-(2-(methoxymethyl)pyrrolidin-1-ylmethyl)ferrocene

: 108-24-7
acetic anhydride

: 173951-66-1,318498-29-2
(S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene

Guidance literature:: In acetic anhydride; (N2); reflux (10 h); addn. of Et2O, washing (aq. NaOH; aq. HCl), drying (Na2SO4), solvent removal (vac.), crystn. (Et2O/CH2Cl2); elem. anal.;

Reference yield: 76.0%

: rac-2-(N,N-dimethylaminomethyl)-1-diphenylphosphanylferrocene

: 108-24-7
acetic anhydride

: 318498-29-2,173951-66-1
rac-[2-(diphenylphosphino)ferrocenyl]methyl acetate

Guidance literature:: In acetic anhydride; reaction flask was flushed with Ar, heating to 100 °C for 2 h; standing at -18 °C overnight, solidifed mixt. was washed thoroughly with MeOH, drying in air;
DOI:10.1039/b204655p

Reference yield: 94.0%

: 173951-66-1,318498-29-2
(S(p))-1-diphenylphosphanyl-2-acetoxymethylferrocene

: (S_p)-(2-diphenylphosphino)hydroxymethylferrocene

Guidance literature:: With KOH; In tetrahydrofuran; methanol; water; (N2); reflux (2 h); evapn. (vac.), treatment with H2O, extn. (Et2O), drying (Na2SO4), evapn.(vac.), crystn. (hexane); elem. anal.;