2,17-dioxo[3,3](4,4'-)biphenylophane

Base Information

• Chemical Name: 2,17-dioxo[3,3](4,4'-)biphenylophane
• CAS No.: 1058140-98-9
• Molecular Formula: C₃₀H₂₄O₂
• Molecular Weight: 416.519
• Mol file: 1058140-98-9.mol

Synonyms:

Chemical Property of 2,17-dioxo[3,3](4,4'-)biphenylophane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2,17-dioxo[3,3](4,4'-)biphenylophane

There total 1 articles about 2,17-dioxo[3,3](4,4'-)biphenylophane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

1,3-bis(4-bromophenyl)propan-2-one (54523-47-6) → 2,17-dioxo[3,3](4,4'-)biphenylophane (1058140-98-9) + C45H36Br2O3 + C60H48Br2O4 + C75H60Br2O5

Guidance literature:

With [2,2]bipyridinyl; bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; cyclo-octa-1,5-diene; In N,N-dimethyl-formamide; at 70 ℃; Schlenk technique; Inert atmosphere; Darkness;

DOI:10.1039/c5cc01654a

upstream raw materials:

1,3-bis(4-bromophenyl)propan-2-one