(HC(C(CH₃)NC₆H₃(CH₃)2)2)GeF

Base Information

• Chemical Name: (HC(C(CH₃)NC₆H₃(CH₃)2)2)GeF
• CAS No.: 382150-86-9
• Molecular Formula: C₂₁H₂₅FGeN₂
• Molecular Weight: 397.031
• Mol file: 382150-86-9.mol

Synonyms:

Chemical Property of (HC(C(CH₃)NC₆H₃(CH₃)2)2)GeF

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (HC(C(CH₃)NC₆H₃(CH₃)2)2)GeF

There total 1 articles about (HC(C(CH₃)NC₆H₃(CH₃)2)2)GeF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(HC(C(CH3)NC6H3(CH3)2)2)GeCl (382150-84-7) + trimethyltin fluoride (420-60-0) → (HC(C(CH3)NC6H3(CH3)2)2)GeF (382150-86-9)

Guidance literature:

In dichloromethane; byproducts: Me3SnCl; under N2, standard Schlenk techniques; soln. of Ge compd. in CH2Cl2 added to stirred suspn. of Me3SnF (molar ratio 1:1.1) in CH2Cl2; stirred at room temp. for 2 d; volatiles removed; extd. with n-hexane; stored at -32°C for 24 h;elem. anal.;

DOI:10.1021/om010358j

upstream raw materials:

(HC(C(CH₃)NC₆H₃(CH₃)2)2)GeCl

trimethyltin fluoride

Refernces