C₂₈H₃₃N₃O

Base Information

Chemical Name:C₂₈H₃₃N₃O
CAS No.:1123543-92-9
Molecular Formula:C₂₈H₃₃N₃O
Molecular Weight:427.59
Hs Code.:

C<sub>28</sub>H<sub>33</sub>N<sub>3</sub>O

Synonyms:

Suppliers and Price of C₂₈H₃₃N₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₃₃N₃O

Chemical Property:

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Technology Process of C₂₈H₃₃N₃O

There total 5 articles about C₂₈H₃₃N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 163210-03-5
tert-butyl 4-[(3-bromophenyl)methylene]piperidine-1-carboxylate

: 1123543-92-9
C₂₈H₃₃N₃O

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / diethyl ether / 72 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

3: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / Reflux

With hydrogenchloride; palladium diacetate; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2008.11.052

Reference yield:

: 584555-96-4
C₁₂H₁₄BrN

: 1123543-92-9
C₂₈H₃₃N₃O

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

2: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / Reflux

With palladium diacetate; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2008.11.052

Reference yield:

: 823-78-9
meta-bromobenzyl bromide

: 1123543-92-9
C₂₈H₃₃N₃O

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 24 h / Reflux

2: sodium hydride / tetrahydrofuran / 4 h / 20 °C

3: hydrogenchloride / diethyl ether / 72 h / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

5: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,4-dioxane / Reflux

With hydrogenchloride; palladium diacetate; sodium hydride; potassium carbonate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; In tetrahydrofuran; 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide; toluene; 2: Horner-Wadsworth-Emmons coupling;
DOI:10.1016/j.bmcl.2008.11.052