2--3-(methoxycarbonyl)benzoic acid

Base Information

Chemical Name:2--3-(methoxycarbonyl)benzoic acid
CAS No.:106589-25-7
Molecular Formula:C₁₆H₁₃NO₆
Molecular Weight:315.282
Hs Code.:

2-<N-(2-carboxyphenyl)amino>-3-(methoxycarbonyl)benzoic acid

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Chemical Property of 2--3-(methoxycarbonyl)benzoic acid

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Technology Process of 2--3-(methoxycarbonyl)benzoic acid

There total 3 articles about 2--3-(methoxycarbonyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2902-65-0
2-iodoyl-1,3-benzenedicarboxylic acid

: 106589-25-7
2--3-(methoxycarbonyl)benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) SOCl₂

2: aq. NaOH / methanol / 1 h / Heating

3: 2.) CuCl, N-ethylmorpholine / 1.) butane-2,3-diol, benzene, 100 deg C, 2.) butane-2,3-diol, benzene, 120 deg C, 2 h

With N-ethylmorpholine;; sodium hydroxide; thionyl chloride; copper(l) chloride; In methanol;
DOI:10.1021/jm00387a013

Reference yield:

: 106589-18-8
Dimethyl 2-iodoisophthalate

: 106589-25-7
2--3-(methoxycarbonyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / methanol / 1 h / Heating

2: 2.) CuCl, N-ethylmorpholine / 1.) butane-2,3-diol, benzene, 100 deg C, 2.) butane-2,3-diol, benzene, 120 deg C, 2 h

With N-ethylmorpholine;; sodium hydroxide; copper(l) chloride; In methanol;
DOI:10.1021/jm00387a013

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 106589-19-9
2-iodo-3-(methoxycarbonyl)benzoic acid

: 106589-25-7
2--3-(methoxycarbonyl)benzoic acid

Guidance literature:: With N-ethylmorpholine;; copper(l) chloride; Yield given. Multistep reaction; 1.) butane-2,3-diol, benzene, 100 deg C, 2.) butane-2,3-diol, benzene, 120 deg C, 2 h;
DOI:10.1021/jm00387a013