tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane

Base Information

Chemical Name:tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane
CAS No.:88035-43-2
Molecular Formula:C₃₄H₄₄P₂U
Molecular Weight:752.7
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane

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Technology Process of tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane

There total 1 articles about tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 80290-55-7
uranium tetrachloride-bis{1,2-bis(dimethylphosphino)ethane}

: 766-04-1
benzyllithium

: 88035-43-2
tetrabenzyluranium 1,2-bis(dimethylphosphino)ethane

Guidance literature:: In diethyl ether; (Ar); C6H5CH2Li (4 equiv) soln. added to complex suspn. at -70°C dropwise with stirring, warmed to 10°C over 2 h, stirred for 1 h at 10°C; evapd., extd. (toluene), filtered, concd., pentane added, cooled to -20°C, ppt. collected, washed with pentane, dried (vac.); elem. anal.;
DOI:10.1021/om00080a023