Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CH(CH₃)OH)

Base Information

• Chemical Name: Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CH(CH₃)OH)
• CAS No.: 110902-17-5
• Molecular Formula: C₂₈H₂₇FeO₃P
• Molecular Weight: 498.341

Synonyms:

Chemical Property of Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CH(CH₃)OH)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CH(CH₃)OH)

There total 1 articles about Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CH(CH₃)OH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

acetyl carbonyl cyclopentadienyl triphenylphosphine iron + acetaldehyde (75-07-0,9002-91-9) → Fe(C5H5)(CO)(P(C6H5)3)(COCH2CH(CH3)OH) (101224-02-6,110902-17-5,110902-18-6,83928-91-0,83997-30-2)

Guidance literature:

With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; N2 atmosphere; a soln. of diisopropylamine in THF added to a soln. of n-butyl lithium in hexane at 0°C; cooled to -42°C; a soln. of Fe-complex in THF added; stirred at -42°C for 90 min; CH3CHO added; warmed to room temp.; aq. NH4Cl added; aq. layer extracted with CH2Cl2;org. solns. dried over Na2SO4; evapd.; chromy. (Al2O3, CH2Cl2); elem. anal.;

DOI:10.1021/ja00280a034

Reference yield: 85.0%

Fe(C5H5)(CO)(P(C6H5)3)(COCH2CH(CH3)OH) (101224-02-6,110902-17-5,110902-18-6,83928-91-0,83997-30-2) → Fe(C5H5)(CO)(P(C6H5)3)(COCH2CHCH3(OCOCH3)) (101223-98-7,101162-89-4)

Guidance literature:

With methyllithium; acetic anhydride; In not given; N2 atmosphere; treatment with MeLi at 0°C and quenching with acetic anhydride;;

DOI:10.1021/ja00280a034

upstream raw materials:

acetaldehyde

Downstream raw materials:

Fe(C₅H₅)(CO)(P(C₆H₅)3)(COCH₂CHCH₃(OCOCH₃))

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