isoarctigenin monoacetate

Base Information

• Chemical Name: isoarctigenin monoacetate
• CAS No.: 74892-43-6
• Molecular Formula: C₂₃H₂₆O₇
• Molecular Weight: 414.455
• Mol file: 74892-43-6.mol

Synonyms:

Chemical Property of isoarctigenin monoacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of isoarctigenin monoacetate

There total 1 articles about isoarctigenin monoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

acetic anhydride (108-24-7) + (8S,8'R)-4-hydroxy-3,3',4'-trimethoxylignano-9,9'-lactone (81446-30-2) → isoarctigenin monoacetate (74892-43-6)

Guidance literature:

In pyridine;

Reference yield:

isoarctigenin monoacetate (74892-43-6) → β-acetylconidendrin monomethyl ether (74861-42-0) + 5-acetoxyisoarctigenin monoacetate (74892-44-7)

Guidance literature:

With lead(IV) acetate; In acetic acid; at 70 - 80 ℃; for 5h;

Reference yield:

isoarctigenin monoacetate (74892-43-6) → β-conidendrin monomethyl ether (74861-43-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 22 mg / acetic acid / 5 h / 70 - 80 °C

2: 4percent KOH / methanol

With potassium hydroxide; In methanol; acetic acid;

upstream raw materials:

acetic anhydride

(8S,8'R)-4-hydroxy-3,3',4'-trimethoxylignano-9,9'-lactone

Downstream raw materials:

β-acetylconidendrin monomethyl ether

5-acetoxyisoarctigenin monoacetate

5-allohydroxymatairesinol dimethyl ether

5-alloacetoxymatairesinol dimethyl ether