[(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2]

Base Information

• Chemical Name: [(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2]
• CAS No.: 1187845-45-9
• Molecular Formula: C₆₀H₅₉Cl₂FeN₃OP₂Pd₂
• Molecular Weight: 1239.69
• Mol file: 1187845-45-9.mol

Synonyms:

Chemical Property of [(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2]

There total 1 articles about [(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

bis[(benzyldimethylamino)chloropalladium(II)] + 1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene (1187845-34-6) → [(μ-1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene)(PdCl(2-[(dimethylamino-κN)methyl]phenyl-κC1))2] (1187845-45-9)

Guidance literature:

In dichloromethane; (Ar); exclusion of daylight; soln. of Pd complex and Fe complex in CH2Cl2 was stirred for 1 h; filtered; filtrate layered with hexane; crystd. by diffusion at 4°C for several d; filtered; washed (hexane); dried (vac.); elem. anal.;

DOI:10.1016/j.jorganchem.2009.04.039

upstream raw materials:

1-(N-[(2-(diphenylphosphino)phenyl)methyl]carbamoyl)-1'-(diphenylphosphino)ferrocene