bis(1,5-cyclooctanediylboryl) telluride

Base Information

• Chemical Name: bis(1,5-cyclooctanediylboryl) telluride
• CAS No.: 161294-55-9
• Molecular Formula: C₁₆H₂₈B₂Te
• Molecular Weight: 369.62
• Mol file: 161294-55-9.mol

Synonyms:

Chemical Property of bis(1,5-cyclooctanediylboryl) telluride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis(1,5-cyclooctanediylboryl) telluride

There total 1 articles about bis(1,5-cyclooctanediylboryl) telluride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

9-chloro-9-borabicyclo{3.3.1}nonane (22086-34-6) + disodium telluride (12034-41-2) + water (7732-18-5) → tellurium (14683-12-6) + bis(9-borabicyclo[3.3.1]nonane) + bis(1,5-cyclooctanediylboryl) telluride (161294-55-9) + bis(1,5-cyclooctanediylboryl) ditelluride (161294-56-0) + 1,1:3,3-bis(1,5-cyclooctandiyl)diboroxane (74744-62-0)

Guidance literature:

anaerobic conditions; the mixture was ground, added to a pyrex ampoule, sealed under vacuum, shaken for 1 min; the temperature was increased to 500 ° C; annealing for 4-10 h at 550 ° C;; cooling to room temperature 2 ° C/min; trituration with THF or methanol;;

Reference yield:

bis(1,5-cyclooctanediylboryl) telluride (161294-55-9) + water (7732-18-5) → tellurium (14683-12-6) + bis(9-borabicyclo[3.3.1]nonane) + 1,1:3,3-bis(1,5-cyclooctandiyl)diboroxane (74744-62-0)

Guidance literature:

In toluene; Ar atmosphere, H2O vapor; (5)B-NMR-monitoring;

upstream raw materials:

9-chloro-9-borabicyclo{3.3.1}nonane

disodium telluride

water

Downstream raw materials:

tellurium

1,1:3,3-bis(1,5-cyclooctandiyl)diboroxane