Technology Process of C21H26O4S2
There total 3 articles about C21H26O4S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 83 percent / piperidine acetate, 3 Angstroem molecular sieves / CHCl3 / 48 h / 20 °C
2: 1.) sodium hydride / 1.) 15 min, 50 deg C, DMF 2.) DMF, 24 h, 65 deg C
With
3 A molecular sieve; piperdinium acetate; sodium hydride;
In
chloroform;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97 percent / H2O2 - AcOH
2: 83 percent / piperidine acetate, 3 Angstroem molecular sieves / CHCl3 / 48 h / 20 °C
3: 1.) sodium hydride / 1.) 15 min, 50 deg C, DMF 2.) DMF, 24 h, 65 deg C
With
3 A molecular sieve; dihydrogen peroxide; piperdinium acetate; sodium hydride; acetic acid;
In
chloroform;
- Guidance literature:
-
With
sodium hydride;
Yield given. Multistep reaction. Yields of byproduct given;
1.) 15 min, 50 deg C, DMF 2.) DMF, 24 h, 65 deg C;