isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside
CAS No.:640722-47-0
Molecular Formula:C₆₁H₆₆O₂₅S
Molecular Weight:1231.25
Hs Code.:

isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

There total 1 articles about isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: C₅₁H₅₆O₂₀S

: 640722-47-0
isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1016/j.carres.2003.08.004

Reference yield:

: 640722-47-0
isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: C₅₈H₆₀O₂₆

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 - 20 ℃; for 3h;
DOI:10.1016/j.carres.2003.08.004

Reference yield:

: 640722-47-0
isopropyl 2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-1-thio-β-D-glucopyranoside

: 640722-49-2
2,3,4,6-tetra-O-benzoyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-2,4,6-tri-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: NIS; TMSOTf / CH₂Cl₂ / 3 h / -20 - 20 °C

2: 998 mg / DBU / CH₂Cl₂ / 3 h / 20 °C

With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane;
DOI:10.1016/j.carres.2003.08.004