Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

Base Information

Chemical Name:Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid
CAS No.:115523-59-6
Molecular Formula:C₅₀H₅₆N₂O₁₇
Molecular Weight:956.998
Hs Code.:

Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

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Chemical Property of Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

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Technology Process of Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

There total 4 articles about Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92052-17-0
[(2S,3R,4R,5S,6R)-6-((2R,3R,4R,5S,6R)-3-Amino-4,5-dihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-2,4-bis-benzyloxy-5-hydroxy-tetrahydro-pyran-3-yl]-carbamic acid benzyl ester

: 115523-59-6
Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dioxane; H₂O / 6 h

2: 4-dimethylaminopyridine / pyridine / 1.5 h

With dmap; potassium carbonate; In 1,4-dioxane; pyridine; water;
DOI:10.1016/S0008-6215(00)90840-1

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 115523-59-6
Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / dioxane; H₂O / 6 h

2: 4-dimethylaminopyridine / pyridine / 1.5 h

With dmap; potassium carbonate; In 1,4-dioxane; pyridine; water;
DOI:10.1016/S0008-6215(00)90840-1

Reference yield:

: 92054-17-6
Benzyl-4-O-acetyl-3-O-benzyl-2-(benzyloxycarbonyl)amino-2-desoxy-6-O-(3,4,6-tri-O-acetyl-2-desoxy-2-phthalimido-β-D-glucopyranosyl)-α-D-glucopyranosid

: 115523-59-6
Benzyl-4-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-6-O-(3,4,6-tri-O-acetyl-2-benzyloxycarbonylamino-2-desoxy-β-D-glucopyranosyl)-2-desoxy-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 1 M NaOMe; 2.) 80 percent hydrazine / 1.) methanol, 45 min; 2.) ethanol, 100 deg C, 2 h

2: K₂CO₃ / dioxane; H₂O / 6 h

3: 4-dimethylaminopyridine / pyridine / 1.5 h

With dmap; sodium methylate; potassium carbonate; hydrazine hydrate; In 1,4-dioxane; pyridine; water;
DOI:10.1016/S0008-6215(00)90840-1