Ph₃PAu(I)-tetracene

Base Information

• Chemical Name: Ph₃PAu(I)-tetracene
• CAS No.: 1228177-66-9
• Molecular Formula: C₃₆H₂₆AuP
• Molecular Weight: 686.543
• Mol file: 1228177-66-9.mol

Synonyms:

Chemical Property of Ph₃PAu(I)-tetracene

Chemical Property:

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Technology Process of Ph₃PAu(I)-tetracene

There total 1 articles about Ph₃PAu(I)-tetracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

(triphenylphosphine)gold(I) chloride (14243-64-2) + 5-bromotetracene (23790-75-2) → Ph3PAu(I)-tetracene (1228177-66-9)

Guidance literature:

With n-BuLi; In tetrahydrofuran; under N2; soln. of n-BuLi added at -78°C to stirred soln. of 5-bromotetracene in THF; stirred at -78°C for 2 h; Ph3PAuCl added; warmed to room temp.; stirred for 12 h; solvent reduced; excess hexane added; filtered; crystd. from filtrate byevapn.; elem. anal.;

DOI:10.1021/om100046h

upstream raw materials:

(triphenylphosphine)gold(I) chloride

5-bromotetracene