(4-Bromophenyl)methyl diethyl phosphite

Base Information

Chemical Name:(4-Bromophenyl)methyl diethyl phosphite
CAS No.:523977-65-3
Molecular Formula:C₁₁H₁₆BrO₃P
Molecular Weight:307.124
Hs Code.:
DSSTox Substance ID:DTXSID901279601

Synonyms:SCHEMBL5953661;GQIYWKDVGPFXOP-UHFFFAOYSA-N;DTXSID901279601;(4-bromophenyl)methyl diethyl phosphite;phosphorous acid-4-bromobenzyl diethylester;523977-65-3

Suppliers and Price of (4-Bromophenyl)methyl diethyl phosphite

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4-Bromophenyl)methyl diethyl phosphite

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:306.00204
Heavy Atom Count:16
Complexity:169

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOP(OCC)OCC1=CC=C(C=C1)Br

Technology Process of (4-Bromophenyl)methyl diethyl phosphite

There total 1 articles about (4-Bromophenyl)methyl diethyl phosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 589-17-3
p-bromobenzyl chloride

: 122-52-1
triethyl phosphite

: 523977-65-3
diethyl (4-bromobenzyl)phosphonate

Guidance literature:: Heating;

Reference yield:

: 523977-65-3
diethyl (4-bromobenzyl)phosphonate

: 3-(4-bromophenyl)-6-(4-hexyloxyphenyl)-4,4,5,5-tetracyanocyclohex-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 1) t-BuOK / 1) THF, 10 min, 2) THF, reflux, 20 min

2: 95 percent / CH₂Cl₂ / 1 h / Heating

With potassium tert-butylate; In dichloromethane;

Reference yield:

: 12093-10-6
ferrocenecarboxaldehyde

: 523977-65-3
diethyl (4-bromobenzyl)phosphonate

: (E)-1-ferrocenyl-2-(4-bromophenyl)ethylene

Guidance literature:: With sodium hydride; In tetrahydrofuran; Fe complex and phosphonate were reacted using suspn. of NaH in THF; recrystd. from methylcyclohexane in presence of I2;
DOI:10.1016/j.jorganchem.2005.01.008