Technology Process of C69H74N6O14
There total 4 articles about C69H74N6O14 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
azelaic acid;
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;
In
acetonitrile;
at 20 ℃;
for 0.166667h;
Inert atmosphere;
C30H31N3O6;
With
triethylamine;
In
acetonitrile;
at 20 ℃;
for 0.666667h;
Inert atmosphere;
DOI:10.1007/s00726-011-0908-0
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 2 h / 20 °C
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 0.17 h / 20 °C / Inert atmosphere
2.2: 0.67 h / 20 °C / Inert atmosphere
3.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
4.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 0.17 h / 20 °C / Inert atmosphere
4.2: 0.67 h / 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1007/s00726-011-0908-0
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: trifluoroacetic acid / dichloromethane / 4 h / 20 °C
2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / acetonitrile / 0.17 h / 20 °C / Inert atmosphere
2.2: 0.67 h / 20 °C / Inert atmosphere
With
O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; trifluoroacetic acid;
In
dichloromethane; acetonitrile;
DOI:10.1007/s00726-011-0908-0
