Technology Process of (3Z)-4,5,6,7-tetrahydro-3-pentylidene-5-phenylisobenzofuran-1(3H)-one
There total 3 articles about (3Z)-4,5,6,7-tetrahydro-3-pentylidene-5-phenylisobenzofuran-1(3H)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: phosphorus tribromide / chloroform
2: diethyl ether
3: sodium acetate; pyridinium chlorochromate / dichloromethane
4: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 20 h / 120 °C / 15201 Torr
With
bis(triphenylphosphine)palladium(II) dichloride; sodium acetate; phosphorus tribromide; triethylamine; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; chloroform; N,N-dimethyl-formamide;
1: Vilsmeier formylation / 2: Grignard reaction;
DOI:10.1007/s10562-010-0457-2
- Guidance literature:
-
Multi-step reaction with 3 steps
1: diethyl ether
2: sodium acetate; pyridinium chlorochromate / dichloromethane
3: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 20 h / 120 °C / 15201 Torr
With
bis(triphenylphosphine)palladium(II) dichloride; sodium acetate; triethylamine; pyridinium chlorochromate;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Grignard reaction;
DOI:10.1007/s10562-010-0457-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium acetate; pyridinium chlorochromate / dichloromethane
2: bis(triphenylphosphine)palladium(II) dichloride; triethylamine / N,N-dimethyl-formamide / 20 h / 120 °C / 15201 Torr
With
bis(triphenylphosphine)palladium(II) dichloride; sodium acetate; triethylamine; pyridinium chlorochromate;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1007/s10562-010-0457-2
