{μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n

Base Information

• Chemical Name: {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n
• CAS No.: 134940-78-6
• Molecular Formula: C₆₄H₅₆FeN₁₂
• Molecular Weight: 1049.08
• Mol file: 134940-78-6.mol

Synonyms:

Chemical Property of {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n

There total 2 articles about {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dicyano-4-ethylbenzene (99276-88-7) → {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n (134940-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: further solvent(s)

2: acetone

In acetone;

Reference yield:

(tetraethylphthalocyaninato)iron(II) (134940-73-1) + 1,4-diisocyano-2,3,5,6-tetramethylbenzene (2999-48-6) → {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n (134940-78-6)

Guidance literature:

In acetone; without moisture and oxygen, reluxed for 3 d; extracted with acetone, dried in vacuo at 50°C, elem. anal.;

Reference yield:

{μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II)}n (134940-78-6) → {μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II) iodine0.9}n (134940-80-0)

Guidance literature:

With iodine; In chloroform; without moisture and oxygen, stirred for 1 h; solvent removed in vacuo, sublimed in vacuo;

upstream raw materials:

(tetraethylphthalocyaninato)iron(II)

1,4-diisocyano-2,3,5,6-tetramethylbenzene

1,2-dicyano-4-ethylbenzene

Downstream raw materials:

{μ-(1,4-diisocyano-2,3,5,6-tetramethylbenzene)(tetraethylphthalocyaninato)iron(II) iodine0.9}n