(CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex

Base Information

Chemical Name:(CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex
CAS No.:131078-92-7
Molecular Formula:C₃₂H₃₄O₃P₂SnW
Molecular Weight:831.128
Hs Code.:

(CO)4(Ph<sub>2</sub>PCH<sub>2</sub>CH<sub>2</sub>PPh<sub>2</sub>)tungsten-hydrido-trimethylstannyl complex

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex

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Technology Process of (CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex

There total 1 articles about (CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 29890-05-9
tetracarbonyl-1,2-bis(diphenylphosphino)ethane-tungsten(0)

: 1631-73-8
trimethylstannane

: 131078-92-7
(CO)4(Ph₂PCH₂CH₂PPh₂)tungsten-hydrido-trimethylstannyl complex

Guidance literature:: In tetrahydrofuran; Irradiation (UV/VIS); (N2); irradiation of (CO)4(dppe)W soln. for 8 h; addn. of HSnMe3 at -20°C; slowly warming to room temp.; 1 h; filtration; removal of solvent in vac.; washing (pentane); recrystn. (CH2Cl2/pentane); elem. anal.;