(η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt

Base Information

Chemical Name:(η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt
CAS No.:97667-02-2
Molecular Formula:C₁₄H₁₀CoNO₃
Molecular Weight:299.231
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Chemical Property of (η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt

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Technology Process of (η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt

There total 1 articles about (η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 97667-00-0
(η5-chloroformylcyclopentadienyl)dicarbonylcobalt

: 97667-02-2
(η5-N-phenylcarbamoylcyclopentadienyl)dicarbonylcobalt

Guidance literature:: With C₆H₅NH₂; In diethyl ether; byproducts: C6H5NH3Cl; (N2 or Ar); soln. of Co complex and excess of aniline was stirred at 25°C for 3,5 h, then water was added; ether layer was sepd., washed with water, dried (MgSO4), filtered and chromd. (alumina, Et2O/pentane 3/1), removal of solvent afforded solid; sublimation at 80°C/E-3 Torr; elem. anal.;
DOI:10.1016/0022-328X(85)87147-3