(Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

Base Information

Chemical Name:(Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide
CAS No.:1334484-46-6
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

Chemical Property:

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Technology Process of (Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

There total 5 articles about (Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1334484-33-1
(E)-N-methoxy-N-methyl-7-phenyl-4-(phenylsulfonyl)hept-4-enamide

: 1334484-46-6
(Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

Guidance literature:: With sodium hydrosulfite; sodium hydrogencarbonate; In ethanol; water; for 4h; optical yield given as %de; Reflux; Inert atmosphere;
DOI:10.1021/ja207944c

Reference yield:

: 82561-76-0
C₁₇H₁₈OS

: 1334484-46-6
(Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / dimethyl sulfoxide; mineral oil / 0.33 h / Inert atmosphere

1.2: Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

3.1: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

4.1: sodium hydrosulfite; sodium hydrogencarbonate / ethanol; water / 4 h / Reflux; Inert atmosphere

With sodium hydrosulfite; dilauryl peroxide; sodium hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; mineral oil;
DOI:10.1021/ja207944c

Reference yield:

: 1334484-19-3
2-fluoro-6-((5-phenyl-2-(phenylthio)pent-1-en-3-yl)oxy)pyridine

: 1334484-46-6
(Z)-N-methoxy-N-methyl-7-phenylhept-4-enamide

Guidance literature:: Multi-step reaction with 3 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C / Inert atmosphere

2: dilauryl peroxide / ethyl acetate / Inert atmosphere; Reflux

3: sodium hydrosulfite; sodium hydrogencarbonate / ethanol; water / 4 h / Reflux; Inert atmosphere

With sodium hydrosulfite; dilauryl peroxide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/ja207944c