C₂₃H₁₉ClN₂

Base Information

Chemical Name:C₂₃H₁₉ClN₂
CAS No.:1335242-72-2
Molecular Formula:C₂₃H₁₉ClN₂
Molecular Weight:358.87
Hs Code.:

C<sub>23</sub>H<sub>19</sub>ClN<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₁₉ClN₂

Chemical Property:

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Technology Process of C₂₃H₁₉ClN₂

There total 2 articles about C₂₃H₁₉ClN₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1749-03-7
N-(4-chlorobenzylidene)-4-methoxyaniline

: 1335243-03-2
C₁₆H₁₆N₂

: C₂₃H₁₉ClN₂

: 1335242-72-2
C₂₃H₁₉ClN₂

Guidance literature:: C₁₆H₁₆N₂; With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In tetrahydrofuran; at 20 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

N-(4-chlorobenzylidene)-4-methoxyaniline; In tetrahydrofuran; at 20 ℃; for 70h; optical yield given as %ee; enantioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1021/ol202361t

Reference yield:

: 41825-73-4
2-bromo-4,6-dimethylaniline

: 388116-27-6
indole-4-boronic acid pinacol ester

: C₂₃H₁₉ClN₂

: 1335242-72-2
C₂₃H₁₉ClN₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: bis-triphenylphosphine-palladium(II) chloride; sodium carbonate / water; N,N-dimethyl-formamide / 4 h / 80 °C / Inert atmosphere

2.1: (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate / tetrahydrofuran / 0.17 h / 20 °C / Molecular sieve; Inert atmosphere

2.2: 70 h / 20 °C / Molecular sieve; Inert atmosphere

With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; bis-triphenylphosphine-palladium(II) chloride; sodium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; 2.1: Pictet-Spengler cyclisation / 2.2: Pictet-Spengler cyclisation;
DOI:10.1021/ol202361t