C₄₄H₅₄N₂O₈SSi

Base Information

Chemical Name:C₄₄H₅₄N₂O₈SSi
CAS No.:1360744-01-9
Molecular Formula:C₄₄H₅₄N₂O₈SSi
Molecular Weight:799.073
Hs Code.:

C<sub>44</sub>H<sub>54</sub>N<sub>2</sub>O<sub>8</sub>SSi

Synonyms:

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Chemical Property of C₄₄H₅₄N₂O₈SSi

Chemical Property:

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Technology Process of C₄₄H₅₄N₂O₈SSi

There total 10 articles about C₄₄H₅₄N₂O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360744-11-1
C₄₄H₅₄N₂O₉SSi

: 1360744-01-9
C₄₄H₅₄N₂O₈SSi

Guidance literature:: C₄₄H₅₄N₂O₉SSi; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.5h;

With carbon disulfide; methyl iodide; In tetrahydrofuran; mineral oil; at 20 ℃; for 3h;

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; Reflux;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-09-7
C₁₂H₁₈O₄

: 1360744-01-9
C₄₄H₅₄N₂O₈SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen iodide / water; toluene / 0.5 h / 0 - 20 °C

1.2: 2 h / Reflux

2.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

4.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

5.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

5.2: 1 h / 0 - 20 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

6.2: 3 h / 20 °C

7.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; hydrogen iodide; tri-n-butyl-tin hydride; sodium hydride; triethylamine; platinum(II) chloride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; toluene; mineral oil; 3.1: Sonogashira coupling / 5.1: Hydroboration reaction / 7.1: Barton-McCombie deoxygenation;
DOI:10.1002/chem.201102101

Reference yield:

: 1360744-10-0
C₇H₉IO₂

: 1360744-01-9
C₄₄H₅₄N₂O₈SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: 1H-imidazole; dmap / dichloromethane / 24 h / 20 °C

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide / 24 h / -78 - 20 °C

3.1: platinum(II) chloride / toluene / 1.45 h / 80 °C

4.1: dimethylsulfide borane complex / tetrahydrofuran / 0 - 20 °C

4.2: 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 20 °C

5.2: 3 h / 20 °C

6.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / Reflux

With 1H-imidazole; dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 2,2'-azobis(isobutyronitrile); dimethylsulfide borane complex; tri-n-butyl-tin hydride; sodium hydride; triethylamine; platinum(II) chloride; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil; 2.1: Sonogashira coupling / 4.1: Hydroboration reaction / 6.1: Barton-McCombie deoxygenation;
DOI:10.1002/chem.201102101