3-(2,4-Dimethylphenyl)-2-methylpropanal

Base Information

Chemical Name:3-(2,4-Dimethylphenyl)-2-methylpropanal
CAS No.:6839-81-2
Molecular Formula:C12H16 O
Molecular Weight:176.2548
Hs Code.:
NSC Number:22268
DSSTox Substance ID:DTXSID30281628

Synonyms:6839-81-2;3-(2,4-dimethylphenyl)-2-methylpropanal;NSC22268;DTXSID30281628;NSC-22268;AKOS013991060

Suppliers and Price of 3-(2,4-Dimethylphenyl)-2-methylpropanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 3-(2,4-Dimethylphenyl)-2-methylpropanal

Chemical Property:

Vapor Pressure:0.0128mmHg at 25°C
Boiling Point:259.7°C at 760 mmHg
Flash Point:117.2°C
Density:0.95g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:176.120115130
Heavy Atom Count:13
Complexity:165

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C=C1)CC(C)C=O)C

Technology Process of 3-(2,4-Dimethylphenyl)-2-methylpropanal

There total 6 articles about 3-(2,4-Dimethylphenyl)-2-methylpropanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 180274-28-6
(+/-)-3-(2,4-dimethylphenyl)-2-methylpropan-1-ol

: 6839-81-2
(+/-)-3-(2,4-dimethylphenyl)-2-methylpropanal

Guidance literature:: With pyridinium chlorochromate; In dichloromethane; for 15h; Ambient temperature;
DOI:10.1002/hlca.19960790418

Reference yield:

: 105984-60-9
2-methyl-3-p-tolylpropan-1-ol

: 6839-81-2
(+/-)-3-(2,4-dimethylphenyl)-2-methylpropanal

Guidance literature:: Multi-step reaction with 4 steps

1: 64 percent / LiBr, toluene-4-sulfonic acid hydrate / 15 h / Ambient temperature

2: 80 percent / AlCl₃ / CH₂Cl₂ / 1 h / 3 - 4 °C

3: 99 percent / hydrogen / 5percent Pd/C / ethyl acetate; ethanol / 15 h / 760 Torr / Ambient temperature

4: 77 percent / pyridinium chlorochromate / CH₂Cl₂ / 15 h / Ambient temperature

With aluminium trichloride; hydrogen; toluene-4-sulfonic acid; pyridinium chlorochromate; lithium bromide; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790418

Reference yield:

: 180274-23-1
(+/-)-1,3,4,5-tetrahydro-4,8-dimethyl-2-benzoxepin

: 6839-81-2
(+/-)-3-(2,4-dimethylphenyl)-2-methylpropanal

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / hydrogen / 5percent Pd/C / ethyl acetate; ethanol / 15 h / 760 Torr / Ambient temperature

2: 77 percent / pyridinium chlorochromate / CH₂Cl₂ / 15 h / Ambient temperature

With hydrogen; pyridinium chlorochromate; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1002/hlca.19960790418