Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate)

Base Information

• Chemical Name: Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate)
• CAS No.: 67407-49-2
• Molecular Formula: C₁₇H₂₁O₃Rh
• Molecular Weight: 376.257

Synonyms:

Chemical Property of Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate)

Chemical Property:

Purity/Quality:

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Technology Process of Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate)

There total 1 articles about Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.7%

bis(ethylene)rhodium acetylacetonate + Allyl cinnamyl ether (80586-92-1,56759-11-6) → Rh(methylallyl cinnamyl ether)(pentane-2,4-dionate) (67407-49-2)

Guidance literature:

In pentane; byproducts: ethylene; addn. of excess diene to Rh-complex (room temp., stirring for 12 h); filtration of first crop of product, concn. of filtrate, trituration with pentane, recrystn. (pentane); elem. anal.;

DOI:10.1039/DT9780000333

upstream raw materials:

Allyl cinnamyl ether

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