trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2]

Base Information

• Chemical Name: trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2]
• CAS No.: 41184-54-7
• Molecular Formula: C₃₆H₂₈As₂NiS₂
• Molecular Weight: 733.284

Synonyms:

Chemical Property of trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2]

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Technology Process of trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2]

There total 1 articles about trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

nickel(II) chloride hexahydrate + 1-AsPh2-2-SHC6H4 (16823-73-7) → trans-[Ni((1-AsPh2-2-SHC6H4)-κ2S,As)2] (1383930-35-5,41184-54-7)

Guidance literature:

With triethylamine; In methanol; (N2) soln. NiCl2*6H2O in MeOH was added to soln. ligand and Et3N in MeOH, heated to reflux for 2 h and stirred overnight; ppt. was filtered, washed with MeOH and crystd. from CH2Cl2-MeOH (4:1) at room temp.; elem. anal.;

DOI:10.1021/ic300002p

upstream raw materials:

1-AsPh₂-2-SHC₆H₄

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