{ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)}

Base Information

Chemical Name:{ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)}
CAS No.:149133-59-5
Molecular Formula:C₄₈H₃₆F₃N₄O₄PRu
Molecular Weight:921.877
Hs Code.:

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Chemical Property of {ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)}

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Technology Process of {ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)}

There total 1 articles about {ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75888-63-0
{ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)CO}

: 149133-59-5
{ruthenium(II)(5,10,15,20-tetra(p-methoxy)phenylporphyrinate)(phosphorus trifluoride)}

Guidance literature:: With trifluorophosphane; In dichloromethane; dissolving Ru complex in dry and argon-degassed CH2Cl2; cooling to -80°C; bubbling PF3 gas trough soln. for 1 min; allowing to warm to 20°C; keeping at this temp. for 4 h; passing Ar through soln. for 10 min;; evapn. of solvent to small volume; addn. of hexane; chromy. on short silica gel column with CHCl3/hexane; recrystn. from CHCl3/hexane; elem. anal.;;
DOI:10.1039/DT9930001167