C₁₃H₁₀ClN₃

Base Information

• Chemical Name: C₁₃H₁₀ClN₃
• CAS No.: 1330064-75-9
• Molecular Formula: C₁₃H₁₀ClN₃
• Molecular Weight: 243.695
• Mol file: 1330064-75-9.mol

Synonyms:

Chemical Property of C₁₃H₁₀ClN₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₁₀ClN₃

There total 3 articles about C₁₃H₁₀ClN₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-1H-indazole (13096-96-3) → C13H10ClN3 (1330064-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide

2: tin(ll) chloride; hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate / dichloromethane; water / pH 9

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; caesium carbonate; tin(ll) chloride; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.02.034

Reference yield:

C13H8ClN3O2 (1330064-83-9) → C13H10ClN3 (1330064-75-9)

Guidance literature:

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; tin(ll) chloride; In dichloromethane; water; pH=9;

DOI:10.1016/j.bmcl.2013.02.034

Reference yield:

4-Fluoronitrobenzene (350-46-9,178603-76-4) → C13H10ClN3 (1330064-75-9)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate / N,N-dimethyl-formamide

2: tin(ll) chloride; hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate / dichloromethane; water / pH 9

With hydrogenchloride; sodium hydrogencarbonate; magnesium sulfate; caesium carbonate; tin(ll) chloride; In dichloromethane; water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2013.02.034

upstream raw materials:

4-chloro-1H-indazole

C₁₃H₈ClN₃O₂

4-Fluoronitrobenzene

Downstream raw materials:

C₂₁H₁₃Cl₂F₃N₄O

C₂₁H₁₄ClF₃N₄O

Refernces