Technology Process of Nmoc-FC
There total 6 articles about Nmoc-FC which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
aq. phosphate buffer;
pH=8;
Inert atmosphere;
DOI:10.1039/c3cc41475b
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 24 h / 0 - 20 °C
2: sodium carbonate / 1,4-dioxane / 12 h / 20 °C / Cooling with ice
3: dicyclohexyl-carbodiimide; dmap / N,N-dimethyl-formamide / 12 h / 0 - 20 °C
4: aq. phosphate buffer / pH 8 / Inert atmosphere
With
dmap; sodium carbonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; 1,4-dioxane; aq. phosphate buffer; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41475b
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dicyclohexyl-carbodiimide; dmap / N,N-dimethyl-formamide / 12 h / 0 - 20 °C
2: aq. phosphate buffer / pH 8 / Inert atmosphere
With
dmap; dicyclohexyl-carbodiimide;
In
aq. phosphate buffer; N,N-dimethyl-formamide;
DOI:10.1039/c3cc41475b