(((CH₃)3C)3PN)3TiC₆H₅

Base Information

Chemical Name:(((CH₃)3C)3PN)3TiC₆H₅
CAS No.:288326-28-3
Molecular Formula:C₄₂H₈₆N₃P₃Ti
Molecular Weight:773.966
Hs Code.:

(((CH<sub>3</sub>)3C)3PN)3TiC<sub>6</sub>H<sub>5</sub>

Synonyms:

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Chemical Property of (((CH₃)3C)3PN)3TiC₆H₅

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Technology Process of (((CH₃)3C)3PN)3TiC₆H₅

There total 4 articles about (((CH₃)3C)3PN)3TiC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 288326-25-0
(((CH₃)3C)3PN)3TiCl

: 591-51-5
phenyllithium

: 288326-28-3
(((CH₃)3C)3PN)3TiC₆H₅

Guidance literature:: In diethyl ether; an excess of Li deriv. reagent added to a soln. of Ti imine under N2; stirred for 12 h at 25°; volatiles removed in vacuo; residual graysolid extd. with hexane, concd., left to stand at 25° for 12 h; ppt. filtered off, dried in vacuo; identified by elem. anal., NMR spectra;
DOI:10.1021/om0002069

Reference yield:

: 256431-07-9
[Ti(NP(C(CH₃)3)3)Cl₃]

: 288326-28-3
(((CH₃)3C)3PN)3TiC₆H₅

Guidance literature:: Multi-step reaction with 2 steps

1: benzene

2: diethyl ether

In diethyl ether; benzene;
DOI:10.1021/om0002069

Reference yield:

: 53561-53-8
1,1,1-tri-tert-butyl-N-(trimethylsilyl)phosphanimine

: 288326-28-3
(((CH₃)3C)3PN)3TiC₆H₅

Guidance literature:: Multi-step reaction with 3 steps

1: toluene

2: benzene

3: diethyl ether

In diethyl ether; toluene; benzene;
DOI:10.1021/om0002069