C₂₉H₄₄IN₅O₄SSi₂

Base Information

Chemical Name:C₂₉H₄₄IN₅O₄SSi₂
CAS No.:1203544-75-5
Molecular Formula:C₂₉H₄₄IN₅O₄SSi₂
Molecular Weight:741.841
Hs Code.:

C<sub>29</sub>H<sub>44</sub>IN<sub>5</sub>O<sub>4</sub>SSi<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₄₄IN₅O₄SSi₂

Chemical Property:

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Technology Process of C₂₉H₄₄IN₅O₄SSi₂

There total 14 articles about C₂₉H₄₄IN₅O₄SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1203544-73-3
((2R,3S,4R,5R)-3,4-bis((tert-butyldimethylsilyl)oxy)-5-(6-((3-iodobenzyl)amino)-9H-purin-9-yl)tetrahydrothiophen-2-yl)methanol

: 1203544-75-5
C₂₉H₄₄IN₅O₄SSi₂

Guidance literature:: With dipyridinium dichromate; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1016/j.bmc.2009.10.011

Reference yield:

: 152006-17-2
2,3-O-isopropylidene-L-lyxono-1,4-lactone

: 1203544-75-5
C₂₉H₄₄IN₅O₄SSi₂

Guidance literature:: Multi-step reaction with 11 steps

1: pyridine / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: sodium tetrahydroborate / methanol / 3 h / 0 - 20 °C

3: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

4: sodium sulfide hydrate / N,N-dimethyl-formamide / 15 h / 100 °C / Inert atmosphere

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

6: triethylamine / acetonitrile; 1,2-dichloro-ethane / 96 h / 80 °C / Inert atmosphere

7: triethylamine / ethanol / 24 h / 20 °C / Inert atmosphere

8: acetic acid / water / 70 °C / Inert atmosphere

9: pyridine / 5 h / 50 °C / Inert atmosphere

10: sodium methylate / methanol / 4 h / 20 °C / Inert atmosphere

11: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; dipyridinium dichromate; sodium sulfide hydrate; sodium methylate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 6: |Pummerer Sulfoxide Rearrangement;
DOI:10.1021/acs.jmedchem.7b00805

Reference yield:

: ((3aR,4S,6aR)-2,2-dimethyl-6-oxotetrahydrofuro[3,4-d][1,3]dioxol-4-yl)methyl benzoate

: 1203544-75-5
C₂₉H₄₄IN₅O₄SSi₂

Guidance literature:: Multi-step reaction with 10 steps

1: sodium tetrahydroborate / methanol / 3 h / 0 - 20 °C

2: dmap; triethylamine / dichloromethane / 0 °C / Inert atmosphere

3: sodium sulfide hydrate / N,N-dimethyl-formamide / 15 h / 100 °C / Inert atmosphere

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / -78 °C / Inert atmosphere

5: triethylamine / acetonitrile; 1,2-dichloro-ethane / 96 h / 80 °C / Inert atmosphere

6: triethylamine / ethanol / 24 h / 20 °C / Inert atmosphere

7: acetic acid / water / 70 °C / Inert atmosphere

8: pyridine / 5 h / 50 °C / Inert atmosphere

9: sodium methylate / methanol / 4 h / 20 °C / Inert atmosphere

10: dipyridinium dichromate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

With pyridine; dmap; sodium tetrahydroborate; dipyridinium dichromate; sodium sulfide hydrate; sodium methylate; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In methanol; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetonitrile; 5: |Pummerer Sulfoxide Rearrangement;
DOI:10.1021/acs.jmedchem.7b00805