C₁₄H₂₂O₃

Base Information

Chemical Name:C₁₄H₂₂O₃
CAS No.:166269-62-1
Molecular Formula:C₁₄H₂₂O₃
Molecular Weight:238.327
Hs Code.:

C<sub>14</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:

Suppliers and Price of C₁₄H₂₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₂₂O₃

Chemical Property:

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Technology Process of C₁₄H₂₂O₃

There total 19 articles about C₁₄H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 166376-61-0
C₁₄H₂₀O₃

: 166269-62-1
C₁₄H₂₂O₃

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 12h;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622104-49-7
C₁₄H₂₀O₃

: 166269-62-1
C₁₄H₂₂O₃

: 1622095-36-6
C₁₄H₂₂O₃

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethanol; at 20 ℃; for 12h; Overall yield = 100%; Overall yield = 6 mg;
DOI:10.1002/ejoc.201402096

Reference yield:

: 1622095-12-8
C₂₀H₁₉NO₅

: 166269-62-1
C₁₄H₂₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 20 h / 20 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 2.5 h / -78 °C / Inert atmosphere

2.2: 11.5 h / -78 - -5 °C

3.1: sodium tetrahydroborate / tetrahydrofuran; water / 18 h / 20 °C

4.1: diisobutylaluminium hydride / dichloromethane; cyclohexane / 2 h / -78 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / ethanol / 12 h / 20 °C

With sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; sodium hexamethyldisilazane; diisobutylaluminium hydride; In tetrahydrofuran; ethanol; dichloromethane; cyclohexane; water; 1.1: |Wittig Olefination;
DOI:10.1002/ejoc.201402096