Technology Process of C35H62N4O6
There total 12 articles about C35H62N4O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux
2: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere
3: dichloromethane / 24 h / 20 °C / Inert atmosphere
4: triethylamine / dichloromethane / 24 h / Reflux; Inert atmosphere
5: hydrogen bromide; phenol / dichloromethane; acetic acid / 0 - 25 °C / Inert atmosphere
6: triethylamine / methanol / 24 h / Inert atmosphere
With
lithium aluminium tetrahydride; hydrogen bromide; triethylamine; phenol;
In
tetrahydrofuran; methanol; dichloromethane; acetic acid;
DOI:10.1007/s11095-010-0197-4
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / dichloromethane / 1 h / -10 °C / Inert atmosphere
2: dichloromethane / 24 h / 20 °C / Inert atmosphere
3: triethylamine / dichloromethane / 24 h / Reflux; Inert atmosphere
4: hydrogen bromide; phenol / dichloromethane; acetic acid / 0 - 25 °C / Inert atmosphere
5: triethylamine / methanol / 24 h / Inert atmosphere
With
hydrogen bromide; triethylamine; phenol;
In
methanol; dichloromethane; acetic acid;
DOI:10.1007/s11095-010-0197-4