[1,1'-biphenyl]-4-ylcarbamoyl azide

Base Information

• Chemical Name: [1,1'-biphenyl]-4-ylcarbamoyl azide
• CAS No.: 1352448-25-9
• Molecular Formula: C₁₃H₁₀N₄O
• Molecular Weight: 238.249
• Mol file: 1352448-25-9.mol

Synonyms:

Chemical Property of [1,1'-biphenyl]-4-ylcarbamoyl azide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [1,1'-biphenyl]-4-ylcarbamoyl azide

There total 1 articles about [1,1'-biphenyl]-4-ylcarbamoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

4-biphenyl-carboxylic acid chloride (14002-51-8) → [1,1'-biphenyl]-4-ylcarbamoyl azide (1352448-25-9) + 1-(4-biphenylyl)-2-tetrazolin-5-one (1352448-27-1)

Guidance literature:

4-biphenyl-carboxylic acid chloride; With sodium azide; tetrachlorosilane; In acetonitrile; at 70 - 80 ℃; for 4h;

With sodium hydrogencarbonate; In water; acetonitrile;

DOI:10.1246/cl.2011.1149

upstream raw materials:

4-biphenyl-carboxylic acid chloride