Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)

Base Information

Chemical Name:Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)
CAS No.:1176086-77-3
Molecular Formula:C₁₇H₁₁Cl₂F₁₀GeN₃
Molecular Weight:590.774
Hs Code.:

Cl<sub>2</sub>Ge(C<sub>6</sub>F<sub>5</sub>NCH<sub>2</sub>CH<sub>2</sub>N(CH<sub>3</sub>)CH<sub>2</sub>CH<sub>2</sub>NC<sub>6</sub>F<sub>5</sub>)

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Suppliers and Price of Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)

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Technology Process of Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)

There total 4 articles about Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 282726-67-4
(C₆F₅NHCH₂CH₂)2NCH₃

: 24422-24-0
{(CH₃)2N}2GeCl₂

: 1176086-77-3
CH₃N(CH₂CH₂NC₆F₅)2GeCl₂

Guidance literature:: In neat (no solvent); (Ar, Schlenk) a mixt. of Ge-compound and amine was heated at 130°C for 25 h, toluene was added at room temp.; filtered, washed with cold diethyl ether and dried in vac.;
DOI:10.1039/b901885a

Reference yield: 54.0%

: 1403585-47-6
GeC₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅

: 10038-98-9
germaniumtetrachloride

: 1176086-77-3
Cl₂Ge(C₆F₅NCH₂CH₂N(CH₃)CH₂CH₂NC₆F₅)

Guidance literature:: In toluene; soln. of GeCl4 in toluene added dropwise to stirred soln. of Ge compd. in toluene at 0°C; stirred at room temp. for 24 h; ppt. removed by filtration; ppt. extd. with toluene; org. solns. combined; volatiles removed in vac.; Et2O added, solid separated by filtration,washed with Et2O, dried under vac.;
DOI:10.1002/ejic.201200363

Reference yield: 48.0%

: 2Li⁽¹⁺⁾*CH₃N(CH₂CH₂NC₆F₅)2^(2-)=Li₂CH₃N(CH₂CH₂NC₆F₅)2

: 10038-98-9
germaniumtetrachloride

: 1176086-77-3
CH₃N(CH₂CH₂NC₆F₅)2GeCl₂

Guidance literature:: In toluene; byproducts: LiCl; (Ar, Schlenk) GeCl4 in toluene was added to a Li-compound in toluene at -78°C with stirring, the soln. was stirred for 24 h at room temp.; ppt. was extd. with toluene, reduced in vol. in vac., diethyl ether was added, filtered, washed with cold diethyl ether, dried in vac.; elem. anal.;
DOI:10.1039/b901885a