tetramethylammonium tris(thiobenzoato-O,S)mercury(II)

Base Information

Chemical Name:tetramethylammonium tris(thiobenzoato-O,S)mercury(II)
CAS No.:189166-07-2
Molecular Formula:C₄H₁₂N*C₂₁H₁₅HgO₃S₃
Molecular Weight:686.282
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetramethylammonium tris(thiobenzoato-O,S)mercury(II)

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Technology Process of tetramethylammonium tris(thiobenzoato-O,S)mercury(II)

There total 1 articles about tetramethylammonium tris(thiobenzoato-O,S)mercury(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

: 98-91-9
thiobenzoic acid

: 75-57-0
tetramethlyammonium chloride

: mercury dichloride

: 189166-07-2
tetramethylammonium tris(thiobenzoato-O,S)mercury(II)

Guidance literature:: With Na; MeOH; In methanol; Ar-atmosphere; addn. of thiobenzoic acid to NaOMe (prepd. from Na in MeOH), addn. to stoich. amt. of HgCl2 soln., stirring with stoich. amt. of Me4NCl for 10 min; extn. into hot aq. MeCN, filtration, crystn. on cooling to 278 K, decantation, washing (MeOH, Et2O), drying (Ar-stream);
DOI:10.1107/S0108270196014692