C₂₉H₂₆B₂F₄N₄O

Base Information

• Chemical Name: C₂₉H₂₆B₂F₄N₄O
• CAS No.: 1375799-65-7
• Molecular Formula: C₂₉H₂₆B₂F₄N₄O
• Molecular Weight: 544.167
• Mol file: 1375799-65-7.mol

Synonyms:

Chemical Property of C₂₉H₂₆B₂F₄N₄O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₆B₂F₄N₄O

There total 4 articles about C₂₉H₂₆B₂F₄N₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C29H29BF2N4O → C29H26B2F4N4O (1375799-65-7)

Guidance literature:

C₂₉H₂₉BF₂N₄O; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; for 1h;

With triethylamine; In dichloromethane; for 0.333333h;

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1039/c2cc30915g

Reference yield:

C17H13BF2N2O2 (1341774-18-2) → C29H26B2F4N4O (1375799-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

2.2: 0.33 h

2.3: 2 h / 20 °C

With trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;

DOI:10.1039/c2cc30915g

Reference yield:

4,4-difluoro-8-(4-methoxyphenyl)-4-bora-3a,4a-diaza-s-indacene → C29H26B2F4N4O (1375799-65-7)

Guidance literature:

Multi-step reaction with 3 steps

1.1: trichlorophosphate / dichloromethane

2.1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

3.2: 0.33 h

3.3: 2 h / 20 °C

With trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; trichlorophosphate; In dichloromethane;

DOI:10.1039/c2cc30915g

upstream raw materials:

C₁₇H₁₃BF₂N₂O₂

2,4-dimethyl-1H-pyrrole