tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾

Base Information

Chemical Name:tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾
CAS No.:72883-60-4
Molecular Formula:C₃₃H₃₀MoO₃P₂
Molecular Weight:632.487
Hs Code.:

tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum<sup>(0)</sup>

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Chemical Property of tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾

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Technology Process of tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾

There total 2 articles about tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 64730-60-5
1,6-bis(diphenylphosphino)-trans-hex-3-ene

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 72883-60-4
tricarbonyl-1,6-bis(diphenylphosphino)-trans-hex-3-ene molybdenum⁽⁰⁾

Guidance literature:: In toluene; Mo complex and org. compd. refluxed in toluene for 2.5 d; cooling, evapn. in vac., recrystn. (CH2Cl2/MeOH); elem. anal.;
DOI:10.1016/S0022-328X(00)87075-8

Reference yield: 72.0%

: 19845-69-3
1,6-bis(diphenylphosphino)hexane

: 13939-06-5,199620-15-0
molybdenum hexacarbonyl

: 72883-60-4
Mo(CO)3((C₆H₅)2PCH₂CH₂CHCHCH₂CH₂P(C₆H₅)2)

Guidance literature:: In decalin; refluxing with stirring for 80 min under dry N2, cooling to -15°C; ppt. filtered, recrystn. from CH2Cl2-MeOH, elem. anal.;