C₃₄H₄₀FN₇O₅

Base Information

Chemical Name:C₃₄H₄₀FN₇O₅
CAS No.:1332639-37-8
Molecular Formula:C₃₄H₄₀FN₇O₅
Molecular Weight:645.734
Hs Code.:

C<sub>34</sub>H<sub>40</sub>FN<sub>7</sub>O<sub>5</sub>

Synonyms:

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Chemical Property of C₃₄H₄₀FN₇O₅

Chemical Property:

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Technology Process of C₃₄H₄₀FN₇O₅

There total 30 articles about C₃₄H₄₀FN₇O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 1332639-37-8
C₃₄H₄₀FN₇O₅

Guidance literature:: Multi-step reaction with 15 steps

1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

3: dmap / dichloromethane / 3 h / 0 °C

4: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

5: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

6: ethyl acetate; diethyl ether

7: lithium borohydride / tetrahydrofuran / 3 h / 0 °C

8: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

9: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

10: copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate / ethanol; water; tert-butyl alcohol

11: trifluoroacetic acid / dichloromethane

12: HATU / 1-methyl-pyrrolidin-2-one

13: trifluoroacetic acid / dichloromethane

14: HATU / 1-methyl-pyrrolidin-2-one

15: trifluoroacetic acid / dichloromethane

With dmap; sodium periodate; lithium borohydride; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tetrabutyl ammonium fluoride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; diethyl ether; ethanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 187039-57-2,335280-19-8
(2S,3S)-1-(tert-butoxycarbonyl)-3-hydroxypyrrolidine-2-carboxylic acid

: 1332639-37-8
C₃₄H₄₀FN₇O₅

Guidance literature:: Multi-step reaction with 23 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 0 - 90 °C

2.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

3.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C

4.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 - 20 °C

5.1: triethylamine / 12 h

6.1: thionyl chloride / dichloromethane / 1 h / -78 °C

6.2: 1 h / -78 °C

7.1: / acetonitrile / 16 h / 20 °C

8.1: hydrogen / ethanol / 1.5 h / 2585.81 Torr

9.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

11.1: dmap / dichloromethane / 3 h / 0 °C

12.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

13.1: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

14.1: ethyl acetate; diethyl ether

15.1: lithium borohydride / tetrahydrofuran / 3 h / 0 °C

16.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

17.1: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

18.1: copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate / ethanol; water; tert-butyl alcohol

19.1: trifluoroacetic acid / dichloromethane

20.1: HATU / 1-methyl-pyrrolidin-2-one

21.1: trifluoroacetic acid / dichloromethane

22.1: HATU / 1-methyl-pyrrolidin-2-one

23.1: trifluoroacetic acid / dichloromethane

With 1H-imidazole; dmap; sodium periodate; lithium borohydride; thionyl chloride; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tetrabutyl ammonium fluoride; hydrogen; sulfur trioxide pyridine complex; sodium hydride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;

Reference yield:

: 184046-78-4
(2S,3S)-1-tert-butyl-2-methyl 3-hydroxypyrrolidine-1,2-dicarboxylate

: 1332639-37-8
C₃₄H₄₀FN₇O₅

Guidance literature:: Multi-step reaction with 22 steps

1.1: 1H-imidazole / dichloromethane / 6 h / 0 - 20 °C

2.1: lithium borohydride / tetrahydrofuran / 3 h / 0 - 20 °C

3.1: triethylamine; sulfur trioxide pyridine complex / dichloromethane; dimethyl sulfoxide / 2 h / 0 - 20 °C

4.1: triethylamine / 12 h

5.1: thionyl chloride / dichloromethane / 1 h / -78 °C

5.2: 1 h / -78 °C

6.1: / acetonitrile / 16 h / 20 °C

7.1: hydrogen / ethanol / 1.5 h / 2585.81 Torr

8.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 6 h / 20 - 45 °C

10.1: dmap / dichloromethane / 3 h / 0 °C

11.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

12.1: sodium periodate / ruthenium(III) trichloride hydrate / 1-methyl-pyrrolidin-2-one; tetrachloromethane; acetonitrile; water / 3.83 h

13.1: ethyl acetate; diethyl ether

14.1: lithium borohydride / tetrahydrofuran / 3 h / 0 °C

15.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C

16.1: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C

17.1: copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate / ethanol; water; tert-butyl alcohol

18.1: trifluoroacetic acid / dichloromethane

19.1: HATU / 1-methyl-pyrrolidin-2-one

20.1: trifluoroacetic acid / dichloromethane

21.1: HATU / 1-methyl-pyrrolidin-2-one

22.1: trifluoroacetic acid / dichloromethane

With 1H-imidazole; dmap; sodium periodate; lithium borohydride; thionyl chloride; sodium azide; copper(ll) sulfate pentahydrate; sodium 2-(1,2-dihydroxyethyl)-4-hydroxy-5-oxo-2,5-dihydro-furan-3-olate; tetrabutyl ammonium fluoride; hydrogen; sulfur trioxide pyridine complex; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; ruthenium(III) trichloride hydrate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; tetrachloromethane; diethyl ether; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; tert-butyl alcohol;