C₆₂H₆₂N₆O₁₃S₂

Base Information

Chemical Name:C₆₂H₆₂N₆O₁₃S₂
CAS No.:1309372-09-5
Molecular Formula:C₆₂H₆₂N₆O₁₃S₂
Molecular Weight:1163.34
Hs Code.:

C<sub>62</sub>H<sub>62</sub>N<sub>6</sub>O<sub>13</sub>S<sub>2</sub>

Synonyms:

Suppliers and Price of C₆₂H₆₂N₆O₁₃S₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of C₆₂H₆₂N₆O₁₃S₂

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₆₂H₆₂N₆O₁₃S₂

There total 8 articles about C₆₂H₆₂N₆O₁₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309371-90-1
N₄-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidenecytidine

: 1309372-09-5
C₆₂H₆₂N₆O₁₃S₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -70 °C

1.2: 1 h / -60 °C

1.3: -20 °C

2.1: sodium tetrahydroborate / ethanol / 0.5 h

3.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C

4.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 h / 23 °C

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C

5.2: 1.5 h / 0 °C

6.1: dichloro-acetic acid; chlorotriisopropylsilane / dichloromethane / 0.75 h

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C

8.1: caesium carbonate; lithium bromide / N,N-dimethyl-formamide / 4 h

With dichloro-acetic acid; dmap; sodium tetrahydroborate; chlorotriisopropylsilane; di-isopropyl azodicarboxylate; caesium carbonate; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; 5.1: Mitsunobu reaction / 5.2: Mitsunobu reaction;
DOI:10.1002/hlca.201000451

Reference yield:

: 1309371-91-2
N₄-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-6-(hydroxymethyl)-2',3'-O-isopropylidenecytidine

: 1309372-09-5
C₆₂H₆₂N₆O₁₃S₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 °C

2.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 h / 23 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C

3.2: 1.5 h / 0 °C

4.1: dichloro-acetic acid; chlorotriisopropylsilane / dichloromethane / 0.75 h

5.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C

6.1: caesium carbonate; lithium bromide / N,N-dimethyl-formamide / 4 h

With dichloro-acetic acid; dmap; chlorotriisopropylsilane; di-isopropyl azodicarboxylate; caesium carbonate; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 3.1: Mitsunobu reaction / 3.2: Mitsunobu reaction;
DOI:10.1002/hlca.201000451

Reference yield:

: 1309371-92-3
N₄-benzoyl-5'-O-[dimethyl(1,1,2-trimethylpropyl)silyl]-2',3'-O-isopropylidene-6-{[(4-methoxyphenyl)(diphenyl)methoxy]methyl}cytidine

: 1309372-09-5
C₆₂H₆₂N₆O₁₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 20 h / 23 °C

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.17 h / 0 °C

2.2: 1.5 h / 0 °C

3.1: dichloro-acetic acid; chlorotriisopropylsilane / dichloromethane / 0.75 h

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 0 °C

5.1: caesium carbonate; lithium bromide / N,N-dimethyl-formamide / 4 h

With dichloro-acetic acid; chlorotriisopropylsilane; di-isopropyl azodicarboxylate; caesium carbonate; triethylamine tris(hydrogen fluoride); N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 2.1: Mitsunobu reaction / 2.2: Mitsunobu reaction;
DOI:10.1002/hlca.201000451