C₅₄H₆₅NO₂

Base Information

• Chemical Name: C₅₄H₆₅NO₂
• CAS No.: 1313995-14-0
• Molecular Formula: C₅₄H₆₅NO₂
• Molecular Weight: 760.116
• Mol file: 1313995-14-0.mol

Synonyms:

Chemical Property of C₅₄H₆₅NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₄H₆₅NO₂

There total 8 articles about C₅₄H₆₅NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-isocyanatooctane (3158-26-7) + C45H48O → C54H65NO2 (1313995-14-0)

Guidance literature:

With dibutyltin dilaurate; In dichloromethane; at 20 ℃;

DOI:10.1039/c1ob05441d

Reference yield:

3,5-diiodo-1-octylbenzene (1313995-06-0) → C54H65NO2 (1313995-14-0)

Guidance literature:

Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

4: dibutyltin dilaurate / dichloromethane / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetrabutyl ammonium fluoride; dibutyltin dilaurate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1: Castro-Stephen-Sonogashira coupling / 2: Castro-Stephen-Sonogashira coupling;

DOI:10.1039/c1ob05441d

Reference yield:

2,6-diiodo-4-octylaniline (1313995-16-2) → C54H65NO2 (1313995-14-0)

Guidance literature:

Multi-step reaction with 5 steps

1.1: sulfuric acid; sodium nitrite / -5 °C

1.2: Reflux

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

3.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.25 h

5.1: dibutyltin dilaurate / dichloromethane / 20 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sulfuric acid; tetrabutyl ammonium fluoride; dibutyltin dilaurate; N-ethyl-N,N-diisopropylamine; sodium nitrite; In tetrahydrofuran; dichloromethane; 2.1: Castro-Stephen-Sonogashira coupling / 3.1: Castro-Stephen-Sonogashira coupling;

DOI:10.1039/c1ob05441d

upstream raw materials:

2,6-diiodo-4-octylaniline

3,5-diiodo-1-octylbenzene

C₁₉H₂₄OSi₂

C₁₃H₈O