C₄₃H₅₈N₂O₉

Base Information

Chemical Name:C₄₃H₅₈N₂O₉
CAS No.:1343505-56-5
Molecular Formula:C₄₃H₅₈N₂O₉
Molecular Weight:746.942
Hs Code.:

C<sub>43</sub>H<sub>58</sub>N<sub>2</sub>O<sub>9</sub>

Synonyms:

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Chemical Property of C₄₃H₅₈N₂O₉

Chemical Property:

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Technology Process of C₄₃H₅₈N₂O₉

There total 11 articles about C₄₃H₅₈N₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₃H₄₇NO₈

: 7524-50-7
methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

: 1343505-56-5
C₄₃H₅₈N₂O₉

Guidance literature:: With 1-ethyl-piperidine; HATU; In acetonitrile; at 0 - 20 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-12-3
C₁₈H₂₈O₄

: 1343505-56-5
C₄₃H₅₈N₂O₉

Guidance literature:: Multi-step reaction with 9 steps

1: 2,6-dimethylpyridine / dichloromethane / 0.75 h / 20 °C

2: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

3: triethylamine / dichloromethane / 0 - 20 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

5: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C

6: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

7: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

8: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

9: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

With 1-ethyl-piperidine; 2,6-dimethylpyridine; dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; HATU; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158

Reference yield:

: 1343505-18-9
C₂₄H₄₂O₄Si

: 1343505-56-5
C₄₃H₅₈N₂O₉

Guidance literature:: Multi-step reaction with 8 steps

1: diisobutylaluminium hydride / dichloromethane / 2 h / -40 - -10 °C

2: triethylamine / dichloromethane / 0 - 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 12 h / 0 - 20 °C

4: dmap; 2,4,6-trichlorobenzoyl chloride; triethylamine / dichloromethane / 7 h / 0 - 20 °C

5: toluene-4-sulfonic acid / methanol / 0.5 h / 20 °C

6: Dess-Martin periodane / dichloromethane / 1 h / 0 - 20 °C

7: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h

8: 1-ethyl-piperidine; HATU / acetonitrile / 12 h / 0 - 20 °C

With 1-ethyl-piperidine; dmap; sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene; 2,4,6-trichlorobenzoyl chloride; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; HATU; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; tert-butyl alcohol;
DOI:10.1016/j.tetlet.2011.08.158