C₂₆H₂₂F₃NO₄

Base Information

Chemical Name:C₂₆H₂₂F₃NO₄
CAS No.:1355483-68-9
Molecular Formula:C₂₆H₂₂F₃NO₄
Molecular Weight:469.46
Hs Code.:

C<sub>26</sub>H<sub>22</sub>F<sub>3</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₂F₃NO₄

Chemical Property:

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Technology Process of C₂₆H₂₂F₃NO₄

There total 10 articles about C₂₆H₂₂F₃NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1343494-04-1
C₁₆H₁₃F₃O

: 1355483-68-9
C₂₆H₂₂F₃NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / acetonitrile / 80 °C

2: potassium permanganate / water / 70 °C

3: O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With potassium permanganate; O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.08.102

Reference yield:

: 1343494-02-9
C₁₆H₁₃F₃O₃

: 1355483-68-9
C₂₆H₂₂F₃NO₄

Guidance literature:: Multi-step reaction with 5 steps

1: trifluorormethanesulfonic acid; trifluoroacetic anhydride / dichloromethane / 10 °C

2: triethylsilane; trifluoroacetic acid / dichloromethane / -10 - 20 °C

3: acetic acid / acetonitrile / 80 °C

4: potassium permanganate / water / 70 °C

5: O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With triethylsilane; potassium permanganate; trifluorormethanesulfonic acid; O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; 1: Friedel Crafts reaction;
DOI:10.1016/j.bmcl.2011.08.102

Reference yield:

: 1343494-03-0
C₁₆H₁₁F₃O₂

: 1355483-68-9
C₂₆H₂₂F₃NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: triethylsilane; trifluoroacetic acid / dichloromethane / -10 - 20 °C

2: acetic acid / acetonitrile / 80 °C

3: potassium permanganate / water / 70 °C

4: O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With triethylsilane; potassium permanganate; O-(1H-6-chlorobenzotriazole-1-yl)-1,1,3,3-tetramethyluronium hexafluorophosphate; acetic acid; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.08.102