1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

Base Information

Chemical Name:1-(Isocyanimino)-1-(4-methoxyphenyl)ethan
CAS No.:94268-33-4
Molecular Formula:C₁₀H₁₀N₂O
Molecular Weight:174.202
Hs Code.:

Synonyms:

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Chemical Property of 1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

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Technology Process of 1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

There total 1 articles about 1-(Isocyanimino)-1-(4-methoxyphenyl)ethan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94268-33-4
1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

Guidance literature:: 4-Methoxy-acetophenon-formyl-hydrazon;

Reference yield: 85.0%

: 94268-33-4
1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

: 7790-38-7
palladium(II) iodide

: 95053-32-0
diiodobis[1-(4-methoxyphenyl)ethylideneisocyanamide]palladium

Guidance literature:: In benzene; all manipulations under N2; addn. of CNNC(Me)C6H4OMe to a suspension ofPdI2 in benzene; stirring at room temp. for 2 h;; ppt. was filtered off and dissolved in a large amt. of warm CH2Cl2; filtration; concn. of the filtrate; crystn. (refrigerator); elem. anal.;;

Reference yield: 57.0%

: 12146-37-1,124717-04-0
(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum⁽⁰⁾

: 94268-33-4
1-(Isocyanimino)-1-(4-methoxyphenyl)ethan

: 95053-29-5
tetracarbonylbis[1-(4-methoxyphenyl)ethylideneisocyanamide]molybdenum

Guidance literature:: In tetrahydrofuran; byproducts: bicyclo[2.2.1]hepta-2,5-diene; all manipulations under N2; a THF soln. of the complex was cooled to -30°C; addn. of a cooled (-30°C) THF soln. of CNNC(Me)C6H4OMe; warmed to room temp.;; evapn. under vac.; extn. with hot petroleum ether until the ext. is only slightly yellow colored; concn.; crystn. on cooling; chromy. (Al2O3, CH2Cl2); crystn. (overlayering of the CH2Cl2 soln. with n-pentane, cooling to 0°C); elem. anal.;;