Technology Process of C29H33N3O6S
There total 4 articles about C29H33N3O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 3 steps
1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h
3: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
With
benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
dichloromethane;
DOI:10.1016/j.bmcl.2013.04.023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 0 - 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h
3: Dess-Martin periodane / dichloromethane / 2 h / 0 - 20 °C
With
water; benzotriazol-1-ol; Dess-Martin periodane; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2013.04.023