Mo(CO)3(2,2'-bipyridine)(PPh₃)

Base Information

Chemical Name:Mo(CO)3(2,2'-bipyridine)(PPh₃)
CAS No.:31265-09-5
Molecular Formula:C₃₁H₂₃MoN₂O₃P
Molecular Weight:598.449
Hs Code.:

Mo(CO)3(2,2'-bipyridine)(PPh<sub>3</sub>)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Mo(CO)3(2,2'-bipyridine)(PPh₃)

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Technology Process of Mo(CO)3(2,2'-bipyridine)(PPh₃)

There total 7 articles about Mo(CO)3(2,2'-bipyridine)(PPh₃) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 603-35-0
triphenylphosphine

: 31265-09-5,15492-26-9,137253-91-9
Mo(CO)3(2,2'-bipyridine)(triphenylphosphine)

Guidance literature:: In tetrahydrofuran; byproducts: CO; Electrolysis; Mo(CO)4(C5H3N)2 and triphenylphosphine added to 0.1 M (CH3CH2CH2CH2)4NPF6 in THF soln., electrolyzed under Ar atm. with exclusion of direct illumination, mercury pool electrode used, electrolysis monitored by dp-polarography; soln. reduced by vac. distn., dild. with benzene, standing for about 30min, pptd. supporting electrolyte filtered off, soln. evapd. to dryness, washed with n-heptane and dried in vacuo;
DOI:10.1016/0022-328X(85)87026-1

Reference yield: 37.0%

: cis-Mo(CO)2(2,2'-bipyridine)2

: 137253-91-9,15492-26-9,31265-09-5
Mo(CO)3(2,2'-bipyridine)(PPh₃)

Guidance literature:: With triphenylphosphine; In tetralin; acetonitrile; PPh3 and tetralin added to acetonitrile soln.-slurry of Mo complex, warmed to 373 K over 3 h, held this temp. for further 5 h, with exclusion of direct light, under N2; evapd. under reduced pressure, pptd. with pentane, filtered, extd. withCH2Cl2, filtered, light petroleum added, after several d isolated; elem. anal.;
DOI:10.1039/DT9820002397

Reference yield:

: 15668-64-1
tetracarbonyl(2,2'-bipyridine)molybdenum

: 31265-09-5,15492-26-9,137253-91-9
Mo(CO)3(2,2'-bipyridine)(triphenylphosphine)

Guidance literature:: With triphenylphosphine; In benzene; byproducts: CO; Irradiation (UV/VIS); irradn. at 395 and 514 nm; 298 K; 1E-4 M Mo(CO)4(C10H8N2); 0.1 M PPh3;