Technology Process of C17H17F3O4
There total 6 articles about C17H17F3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; triethylamine;
In
dichloromethane;
at 20 ℃;
for 0.833333h;
Overall yield = 98 %; Overall yield = 33 mg;
Inert atmosphere;
DOI:10.1002/ejoc.201200704
- Guidance literature:
-
Multi-step reaction with 6 steps
1: bromine / chloroform / 0 °C
2: potassium hydroxide / 2,2'-[1,2-ethanediylbis(oxy)]bisethanol / 180 °C
3: palladium diacetate; p-benzoquinone; manganese(IV) oxide; lithium acetate dihydrate / pentane / 72 h / 20 °C
4: potassium carbonate; methanol
5: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
6: dmap; triethylamine / dichloromethane / 0.83 h / 20 °C / Inert atmosphere
With
methanol; dmap; manganese(IV) oxide; lithium acetate dihydrate; bromine; palladium diacetate; potassium carbonate; Dess-Martin periodane; triethylamine; p-benzoquinone; potassium hydroxide;
In
dichloromethane; chloroform; pentane; 2,2'-[1,2-ethanediylbis(oxy)]bisethanol;
DOI:10.1002/ejoc.201200704
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate; methanol
2: Dess-Martin periodane / dichloromethane / 3 h / 20 °C
3: dmap; triethylamine / dichloromethane / 0.83 h / 20 °C / Inert atmosphere
With
methanol; dmap; potassium carbonate; Dess-Martin periodane; triethylamine;
In
dichloromethane;
DOI:10.1002/ejoc.201200704
